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Integrated H 2 O peak intensities were then fitted to an exponential decay with an apparent T 1 decay, and extrapolated based on fittings to the time of the water injection. This extrapolated intensity was normalized by the thermal equilibrium value and plotted as percent polarization of the protons. 2D HyperW NMR spectra were acquired using the 1 H– 15 N HMQC sequence given in Figure S2 of

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